In this work, we prompted to extend the basis of the HPSAM
to kinetic data of voltammetric measurements. Adsorptive linear
sweep voltammetry of Sb(III) and Sb(V) complexes with pyrogallol
(py) was selected as a representative example of highly overlapped
voltammograms. The obtained results showed that the HPSAM in
combination to electroanalytical techniques is a powerful method
with high sensitivity and selectivity, for simultaneous determination
of Sb(III) and Sb(V) in aqueous media.