After 30 min stirring the autoclave was capped and heated at 130 C for 3 days.Then the product was washed three times with acetone. As-synthesized NH2-MIL-101(Al) was activated with methanol under reflux overnight and evacuated at 200 C for 16 h.
After 30 min stirring the autoclave was capped and heated at 130 C for 3 days.Then theproduct was washed three times with acetone. As-synthesized NH2-MIL-101(Al) was activated with methanol under reflux overnight and evacuated at 200 C for 16 h.