For sample preparation, the following equipment was used: IKA® Vortex Genius 3 (IKA® – Werke GmbH & CO.KG, Germany) and centrifuge Rotanta 460R (Hettich GmbH & Co.KG, Tuttlingen, Germany). Tecan Sunrise Absorbance Reader (Tecan Austria GmbH, Salzburg, Austria) was used for measured of optical density at 450 nm.