conditions were: temperature, 150 C; pressure 1500 psi; number of extraction cycles, 1; preheat time, 3 min; heat time, 5 min; static time 10 min; flush volume 60% and purge time, 60 s.
conditions were: temperature, 150 C; pressure 1500 psi; number of extraction cycles, 1; preheat time, 3 min; heat time, 5 min; static time 10 min; flush volume 60% and purge time, 60 s.