in which Cu nanoparticles were embedded in the TiO2, and these were active for the H2 production from glycerol and water under visible light irradiation conditions [10]. The doping of NiOx onto the surface of TiO2 is effective for the preparation of p-type (NiOx)–n-type (TiO2) junction [13]. Such NiOx-doped TiO2 catalysts were recently reported to show good performance of photocatalytic degradation of organic compounds of methyl orange [14], methylene blue [15], and 2-naphthol and p-cresol [16]. In the present work, the authors prepared NiOx/TiO2 catalysts by conventional impregnation and tested their performance in photocatalytic H2 production from a mixture of glycerol and water under UV/vis irradiation conditions. We could find few published study that has considered the use of NiOx/TiO2 photo-sensitive materials for such a H2 production from biomass derived compounds.