Electrochemical impedance spectroscopy (EIS) was performedin the frequency range from 104to 10−1Hz with an ac perturbationof 0.005 V. The measurement potential for each sample was therespective oxidation peak potential. To assure steady state conditions, the electrode was polarized at the measurement potentialfor 3 min. The electrolyte was the same as described above for thecyclic voltammetry experiment.