Thirty minute extraction, with previous 20 min of equilibrium time at 32 °C, and 10 min of thermal desorption at 250 °C in the GC/MS injection port were found sufficient to obtain chromatograms with peaks of good intensity and resolution.
Thirty minute extraction, with previous 20 min of equilibrium time at 32 °C, and 10 min of thermal desorption at 250 °C in the GC/MS injection port were found sufficient to obtain chromatograms with peaks of good intensity and resolution.