Pure and Pb2+doped Ba2Be2B2O7materials were prepared by a solution combustion synthesis method.The phase analysis of all synthesized materials was carried out using the powder XRD. The synthesizedphosphors were investigated using spectrofluorometer at room temperature. The excitation and emis-sion bands of Ba2Be2B2O7:Pb2+were observed at 284 and 396 nm, respectively. The dependence of theemission intensity on the Pb2+concentration for the Ba2Be2B2O7was studied in detail. It was observedthat the concentration quenching of Pb2+in Ba2Be2B2O7is 0.04 mol. The Stokes shifts of Ba2Be2B2O7:Pb2+phosphor were calculated to be 9959 cm