Phenomenex (5 μm C18(2) 100 Å, LC Column 250 × 4.6 mm, Ea,
Phenomenex, USA) and Cyano (80 Å, 5 μm, 4.6 mm × 250 mm,
Spherisorb Cyano (CN) Column, Waters Corporation, USA) columns
were used to determine concentrations of flavonoids and limonin, respectively
Phenomenex (5 μm C18(2) 100 Å, LC Column 250 × 4.6 mm, Ea,Phenomenex, USA) and Cyano (80 Å, 5 μm, 4.6 mm × 250 mm,Spherisorb Cyano (CN) Column, Waters Corporation, USA) columnswere used to determine concentrations of flavonoids and limonin, respectively
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