This method provides procedures for the determination of free carbonyl compounds in
various matrices by derivatization with 2,4-dinitrophenylhydrazine (DNPH). The method utilizes high
performance liquid chromatography (HPLC) with ultraviolet/visible (UV/vis) detection to identify and
quantitate the target analytes. This method includes two procedures encompassing all aspects of
the analysis (extraction to determination of concentration). Procedure 1 is appropriate for the
analysis of aqueous, soil and waste samples and stack samples collected by Method 0011.
Procedure 2 is appropriate for the analysis of indoor air samples collected by Method 0100. The list
of target analytes differs by procedure. The appropriate procedure for each target analyte is listed