By using solid state reaction method ZnO nanomaterials are prepared in the presence of various stabilizers [18–20]. Recently zinc oxide nanorods are successfully prepared under solid state reaction method using Sodium Lauryl Sulphate (SLS) as the stabilizing agent via sonochemical method at room temperature [21,22]. It is observed that the SLS and ultrasonic both plays a vital role on the growth of ZnO nanostructure. The physical and chemical effects generate d by acoustic cavitation can be expected to significantly influence the properties of doped materials [23,24]. Ultrasound is very useful in the synthesis of a wide range of nanostructured materials, including high-surface area transition metals, alloys, carbides, oxides and colloids. Therefore, the present work