The crystallization,microstructure,microhardnessandtheoreticalmachinabilityhavebeeninvestigatedbyDTA,XRD,SEMand
Microhardness Indenterofresultingglass-ceramics.TwodistinctcrystallizationexothermsintheDTAcurveareobservedandresolved.
The firstpeakcorrespondstotheinitialformationofpotassiumfluorophlogopiteandthesecondisduetotheformationofbarium
fluorophlogopite. Theactivationenergyforprecipitationofeachcrystallinephasehasbeenevaluated,andthecrystallizationmechanism
has beenstudied.DTAanalyseswereconductedatdifferentheatingratesandtheactivationenergywasdeterminedgraphicallyfrom
Kissinger andOzawaequation.Theaverageactivationenergyiscalculatedas276KJ/molforthefirstand366KJ/molforthesecond
crystallization peak.TheAvramiexponentforfirstandsecondcrystallizationpeaktemperaturedeterminedbyAugisandBennett
method isfoundtobe3and3.9,respectively.Theresultsindicatethatthegrowthofmicaisatwoandthreedimensionalprocess,
controlled bythecrystal-glassinterfacereaction.TheVicker’shardnessdecreasedsteadilyatintermediateheattreatmenttemperature
with theformationofbariumandpotassiumfluorophlogopitephase,butthedecreaseinhardnessismorerapidathighertemperature
with thedevelopmentofaninterconnected‘houseofcards’microstructure.
& 2012 PublishedbyElsevierLtdandTechnaGroupS.r.l.
การตกผลึก , โครงสร้างจุลภาค microhardnessandtheoreticalmachinabilityhavebeeninvestigatedbydta , XRD , semand
ความแข็ง indenterofresultingglass เซรามิก twodistinctcrystallizationexothermsinthedtacurveareobservedandresolved .
firstpeakcorrespondstotheinitialformationofpotassiumfluorophlogopiteandthesecondisduetotheformationofbarium fluorophlogopite .ได้ทำการศึกษา theactivationenergyforprecipitationofeachcrystallinephasehasbeenevaluated andthecrystallizationmechanism
, .
dtaanalyseswereconductedatdifferentheatingratesandtheactivationenergywasdeterminedgraphicallyfrom คิสซินเจอร์ andozawaequation . theaverageactivationenergyiscalculatedas276kj / molforthefirstand366kj / molforthesecond
ยอดการตกผลึกtheavramiexponentforfirstandsecondcrystallizationpeaktemperaturedeterminedbyaugisandbennett
วิธี isfoundtobe3and3.9 ตามลำดับ theresultsindicatethatthegrowthofmicaisatwoandthreedimensionalprocess
, ควบคุม bythecrystal glassinterfacereaction . thevicker'shardnessdecreasedsteadilyatintermediateheattreatmenttemperature
theformationofbariumandpotassiumfluorophlogopitephase ด้วย ,butthedecreaseinhardnessismorerapidathighertemperature
กับ thedevelopmentofaninterconnected'houseofcards'microstructure .
& 2012 publishedbyelsevierltdandtechnagroups . .
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