The obtained values of LODm of 3 or 6 μg kg-1 and LOQm of 10 or 20 μg kg-1 were comparable with EU MRLs (10 to 50 μg kg-1) and Brazil MRLs (10 to 20 μg kg-1), except for fipronil with a MRL of 10 μg kg-1 that is below the LOQm of 20 μg kg-1. However, the LODm for fipronil (6 µg kg-1) is suitable for detection in honey samples. It can be concluded that the proposed method allows good detectability, enabling the application of this method in real samples.