Peanut shells were used as a precursor to prepare activated carbon for medical use via CO2 activation in a hightemperature
fluidised bed reactor. The influence of the activation time and activation temperature on the yield
and adsorption capacity of the activated carbon, which were estimated using methylene blue (MB) and
phenazone adsorption, was studied. The activated carbon microstructure was assessed based on N2 adsorption,
scanning electron microscopy, and Fourier transform infrared spectroscopy while the adsorption kinetics was
evaluated usingMB dye. In this study, the optimised conditions, activation temperature of 900 °C and activation
time of 5 h, produced 225.8 mg g−1 MB, 421.5 mg g−1 phenazone uptake and 26.15% yield. At the optimised
conditions, a 1060 m2 g−1 Brunauer–Emmett–Teller specific surface area and 0.8021 cm3 g−1 total pore volume
were obtained for the activated carbon samples, and the presence of carboxyl, hydroxyl and alkyl functional
groups was detected. The investigation of MB adsorption on the prepared activated carbon indicated that the
adsorption kinetics process closely follows a pseudo-second-order chemisorption model. Compared with the
quality index of British Pharmacopoeia and the United States Pharmacopoeia standards for activated carbon,
this peanut shell-based activated carbon preparation was suitable for medicinal use.