3. Sample Handling and Preservation
Use resistant-glass or plastic bottles, provided that the material in suspension does not adhere to container walls. Begin analysis as soon as possible because of the impracticality of preserving the sample. Refrigerate sample at 4°C up to the time of analysis to minimize microbiological decomposition of solids. Preferably do not hold samples more than 24 h. In no case hold sample more than 7 d. Bring samples to room temperature before analysis.