Catalytic wet peroxide oxidation
The experimental set-up shown in Fig. 1 mainly consists of a
reactor, a condenser and suitable measuring devices for temperature,
pressure, and air flow rate. The main part of the system was
a 500mL (h = 500mm; D= 35mm) stainless steel reactor equipped
with an electrical wires wrapped around, a temperature controller
(PID-1/32 DIN model), and a pressure indicator. The condenser
mounted at the top of the reactor was used to condense the vapors
formed during the reaction and to send the condensate back to the
reactor. The experimental setup has been explained elsewhere in
detail [14].