Collection of Sulfur Solution- Rinse the interior of the
bomb, the oil cup, and the inner surface of the bomb cover with
a fine jet of water, and collect the washings in a 600-mL beaker
having a mark to indicate 75 mL. Remove any precipitate in
the bomb by means of a rubber policeman. Wash the base of
the terminals until the washings are neutral to the indicator
methyl red. Add 10 mL of saturated bromine water to the
washings in the beaker. (The volume of the washings is
normally in excess of 300 mL.) Place the sample cup in a
50-mL beaker. Add 5 mL of saturated bromine water, 2 mL of
HCI, and enough water just to cover the cup. Heat the contents