This study aimed at making of rayon pulp (dissolving pulp) of four species of bamboo such as Apus (Gigantochloa apus), Petung (Dendrocalamus asper), Mayan (Gigantochloa robusta) and Sembilang (Dendrocalamus giganteus) by the pre-hydrolysis-Kraft process and bleaching of pulp with environmental friendly technology (Elemental Chlorine Free and enzyme). The results are compared with Indonesian standard specification for dissolving pulp (SNI 0938:2010, Pulp Rayon).