The main objective of the present study is to establish an environmentally friendly method for the preparation of regenerated cellulose materials from low-value agricultural residues replacing the traditional high-grade dissolving pulp. In this article, the cornhusk was used to prepare cellulose, and the obtained cornhusk cellulose (CC) was dissolved and regenerated in AmimCl and EmimAc solvents, and the films were cast from the resulting solutions. The details of the dissolution process of cellulose in the two ILs, and the formation of the regenerated cellulose materials are presented in this article. To evaluate the suitability of CC for industrial applications,
the properties of regenerated cornhusk cellulose (RCC) were compared with regenerated cellulose from high-grade dissolving WP. Moreover, the recovery of ILs after the dissolution and regeneration is also discussed.