Hydrolysis is necessary to convert starches to fermentable sugars. The cell degradation of carbohydrates to fermentable sugar is basically done with the hydrolysis process by making solution with Sulphuric Acid.The termJAcid HydrolysisK is also applied to certain nucleophilic addition reactions, such as in the acid catalyzed hydrolysis of nitriles to amides. Acid hydrolysis doesnot usually refer to the acid catalyzed addition of the elements of water to double or triple bonds by electrophilic addition as may originate from a hydration reaction.For our work purpose we have made three sample solutions with the variation of Sulphuric acid percentage. Every sample solution is 500 ml solution. This solution was made with algal powder and distilled water. Three samples were made with 1%, 1.5% & 2% sulphuric acid by weight percentage.