2. Experimental
2.1. Starting materials
Zr(OPr)4 with a concentration of 70 wt% was supplied by the Shanghai Jingchun Reagents Co. Ltd., Shanghai, China. H3BO3, C12H22O11, and AcOH were supplied by the Lanyi Reagents Co. Ltd., Beijing, China. The grade of all the above reagents was analytical.