This work presented a simple and green method for the extraction of the carbamates from dry rice samples.
The proposed method combined MASE with solid phase extraction (SPE).
Parameters affecting extraction efficiency were investigated and optimised.
The results obtained by the optimised MASE–SPE were compared with those obtained by traditional steam extraction andSoxhlet extraction.
Finally, this proposed method was applied on determination of rice samples which were obtained from different production areas.