In this study, a rapid, easy, green, sensitive, and cost-effectiveMSPE–HPLC method was established for simultaneousdetermination of 11 PAEs in plastic bottled beverages withdifferent matrixes. The m-MWCNTs were a satisfactory sorbentfor MSPE because of their strong adsorption capacity for PAEs.The developed method is suitable for the analysis of trace PAEsin beverages.