In this study, the most carcinogenic 4 PAHs were selected and monitored as suitable markers for PAHs in food. We investigated the effects of grilling procedures on the levels of PAHs in grilled foods by sampling meat drippings and smoke adhering to the surface of meats, and the effect of cooking with charcoal at different combustive temperatures. In this way, the obtained results can be used not only to understand PAH formation in grilled meats, but also to establish improved cooking practices.