The samples previously held at 4 °C during storage were inserted into the pressurizing chamber filled with water at 15 ± 1 °C and exposed to a pressure of 500 MPa for 5 min.
The samples previously held at 4 °C during storage were inserted into the pressurizing chamber filled with water at 15 ±1 °C and exposed to a pressure of 500 MPa for 5 min.