The results of the current study indicate that DB-FFAP column can also be used for analysing of FAMEs. During 44 min, most of the peaks of the FAMEs exhibited excellent peak symmetry and DB-FFAP column was selected for further study.The tests of two inlet temperatures (220 and 250 C). at the start of the optimization of this GC method indicated that at the inlet temperature of 220 C, some FAMEs with high boiling points could not be eluted as the energy was too low to vaporize. Therefore at the inlet temperature of 250 C, the recoveries of saturated fatty acids were improved as the peak areas were increased and no thermal degradation was observed. Hence, the inlet temperature of 250 C was chosen for further optimization.