The optimal experimental parameters for assay of this complex are: carbonate supporting electrolyte pH 8, accumulation time 30 s,
accumulation potential −0.1 V, scan rate 200 mV s−1, pulse amplitude 80 mV, frequency 40 Hz, surface area of working electrode
0.6 mm2 and convection rate 1000 rpm. T
The optimal experimental parameters for assay of this complex are: carbonate supporting electrolyte pH 8, accumulation time 30 s,accumulation potential −0.1 V, scan rate 200 mV s−1, pulse amplitude 80 mV, frequency 40 Hz, surface area of working electrode0.6 mm2 and convection rate 1000 rpm. T
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