The left arm of the apparatus was attached to a 250-mL round-bottom solvent flask containing 80 mL of distilled water, 2 mL of diluted sulphuric acid and 120 mL of diethyl ether.
The left arm of the apparatus was attached to a 250-mL round-bottom solvent flask containing 80 mL of distilled water, 2 mL of diluted sulphuric acid and 120 mL of diethyl ether.