Initially, we began our study with the reaction of styrene (1a) and Selectfluor (2a) in the presence of 2 equiv of K2S2O8 to provide 3a in 9% yield under an Ar atmosphere (Table 1, entry 1).
Initially, we began our study with the reaction of styrene(1a) and Selectfluor (2a) in the presence of 2 equiv ofK2S2O8 to provide 3a in 9% yield under an Ar atmosphere(Table 1, entry 1).