A mechanically durable and scalable superhydrophobic coating was fabricated by combining the advantages of both bottom-up and top-down approaches into a one-pot, one-step application method.
This is achieved by spray coating a solution consisting of silica nanoparticles,which are embedded within epoxy resin, onto a heated substrate to rapidly drive both solvent evaporation and curing simultaneously. By maintaining a high substrate
temperature, the arrival of spray-delivered micrometer-sized droplets are rapidly cured onto the substrate to form surface microroughness, while simultaneously, rapid solvent evaporation within each droplet results in the formation of a nanoporous structure. SEM, dual-beamFIB, and cross-sectional TEM/EDAX elementalmapping were used to confirm both the chemistry and the requisitemicro- and nano-porositywithin the coating structure requisite for superhydrophobicity.
The resultant coatings exhibit contact angles greater than 150° (153.8°±0.8°) and roll-off angles of 8°± 2°, with a coating hardness of 6H on the pencil hardness scale, and a rating of 5 on an ASTM crosshatch test.
A mechanically durable and scalable superhydrophobic coating was fabricated by combining the advantages of both bottom-up and top-down approaches into a one-pot, one-step application method. This is achieved by spray coating a solution consisting of silica nanoparticles,which are embedded within epoxy resin, onto a heated substrate to rapidly drive both solvent evaporation and curing simultaneously. By maintaining a high substratetemperature, the arrival of spray-delivered micrometer-sized droplets are rapidly cured onto the substrate to form surface microroughness, while simultaneously, rapid solvent evaporation within each droplet results in the formation of a nanoporous structure. SEM, dual-beamFIB, and cross-sectional TEM/EDAX elementalmapping were used to confirm both the chemistry and the requisitemicro- and nano-porositywithin the coating structure requisite for superhydrophobicity. The resultant coatings exhibit contact angles greater than 150° (153.8°±0.8°) and roll-off angles of 8°± 2°, with a coating hardness of 6H on the pencil hardness scale, and a rating of 5 on an ASTM crosshatch test.
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