84 Bring the temperature of the distillate to about 20 C,add 3.85N HCl to the 250-mL mark and mix thoroughly. Pipet 5.0 mL of the distillate into a 50-mL volumetric flask. Add 25.0 mLof orcinol reagent,mix, and place the flask in a water bath at 25 t I°C.