Infrared spectroscopy, a vibrational spectroscopic method coupled with chemometric techniques has emerged as an analytical technique to quantify quality traits in oilseeds. Although, nuclear magnetic resonance (NMR), also a nondestructive technology for estimation of oil content in oilseeds has reduced the analysis time significantly but not considered enough for meeting the market requirements (Panford and de Man, 1990). Earlier, Panford et al. (1988) reported estimation of oil content in ground Safflower achne using monochromator based NIR spectrometer. Elfadl et al. (2010) also reported NIRS calibration model for estimation of oil content in ground samples of Safflower.