Design/methodology/approach: The powder test piece obtained from the input amorphous ribbon in high- energy ball milling. The diffraction examinations and examinations of thin foils were made on the JEOL JEM 200CX transmission electron microscope. Observations of the structure of powders were made on the Opton DSM-940 scanning electron microscope. The X-ray tests were realized with the use of the XRD 7 SEIFERT- FPM diffractometer.