All extractions were performed using 10.0 ± 0.010 g of raw material, constant CO2 flow of 3.00 l/min for 91 min and a solvent/raw material S/F ratio (w/w) of 46. The supercritical extractions were performed at different temperature and pressure values; 40, 50, and 60 °C and 100, 200 and 300 bar, respectively (Table 1). After extraction, the collection bottles, kept at 5 ± 1 °C during extraction, were freed of residual CO2, hermetically re-sealed, isolated from direct light, and stored under refrigeration (Metalfrio Freezer) until its subsequent analysis.