The resulting organic inorganic hybrid LDH materials exhibit a layered structure well organized with the presence of pronounced basal reflections up to seventh to tenth order. Additionally the observed reflections at 2θ close to 35° and 61° were consistent with the formation of a LDH phase, and associated to (101) and (110) diffraction reflections respectively, this in the rhombohedral symmetry adopting the space group R-3 m to describe LDH structure. The reflections at low 2θ values (Fig. 2a) were depicted by enlarging the corresponding angular domain.