Electrochemical impedance spectroscopy (EIS) was performedin the frequency range from 104to 10−1Hz with an ac perturbation of 0.005 V. The measurement potential for each sample was the respective oxidation peak potential. To assure steady state conditions, the electrode was polarized at the measurement potentialf or 3 min. The electrolyte was the same as described above for the cyclic voltammetry experiment.